Institute of Electrical Engineering and Measurement Technology, Department
of Sensors and Measurement Technology, Leibniz Universität Hannover,
30167 Hannover, Germany
Ansgar T. Kirk
Institute of Electrical Engineering and Measurement Technology, Department
of Sensors and Measurement Technology, Leibniz Universität Hannover,
30167 Hannover, Germany
Jens Oermann
Institute of Electrical Engineering and Measurement Technology, Department
of Sensors and Measurement Technology, Leibniz Universität Hannover,
30167 Hannover, Germany
Stefan Zimmermann
Institute of Electrical Engineering and Measurement Technology, Department
of Sensors and Measurement Technology, Leibniz Universität Hannover,
30167 Hannover, Germany
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Electron capture detectors (ECDs) are widely used for the detection of electron affine substances such as pesticides or chlorofluorocarbons. In this work we present a new non-radioactive ECD and investigate the analytical performance depending on the operating parameters. We achieved limits of detection for 1,1,2-trichloroethane and sevoflurane, which are comparable to radioactive ECDs. Furthermore, a pulsed collector voltage mode was implemented, leading to an extended linear range.
Electron capture detectors (ECDs) are widely used for the detection of electron affine...