Articles | Volume 7, issue 2
J. Sens. Sens. Syst., 7, 621–625, 2018
https://doi.org/10.5194/jsss-7-621-2018

Special issue: Sensors and Measurement Systems 2018

J. Sens. Sens. Syst., 7, 621–625, 2018
https://doi.org/10.5194/jsss-7-621-2018

Regular research article 06 Dec 2018

Regular research article | 06 Dec 2018

Highly sensitive coulometric titration of oxygen for the characterization of solid materials at elevated temperatures

Alexander Herms et al.

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Latest update: 25 Jan 2022
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Short summary
For the understanding of new materials, especially oxides, oxygen exchange of such materials and its consequences for their properties are of high interest. For this purpose a new setup for oxygen solid electrolyte coulometry with electrochemical cells made of yttria-stabilized zirconia (YSZ) is presented. It could be shown that this setup enables the measurement of exchanged oxygen from the picomol up to the higher nanomol range with a precision which was not achieved so far.