Articles | Volume 2, issue 2
https://doi.org/10.5194/jsss-2-95-2013
© Author(s) 2013. This work is distributed under
the Creative Commons Attribution 3.0 License.
the Creative Commons Attribution 3.0 License.
https://doi.org/10.5194/jsss-2-95-2013
© Author(s) 2013. This work is distributed under
the Creative Commons Attribution 3.0 License.
the Creative Commons Attribution 3.0 License.
Improvement of the sensitivity of a conductometric soot sensor by adding a conductive cover layer
P. Bartscherer
Robert Bosch GmbH, Robert-Bosch-Platz 1, 70839 Gerlingen-Schillerhöhe, Germany
R. Moos
Bayreuth Engine Research Center (BERC), University of Bayreuth, 95447 Bayreuth, Germany
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Thomas Wöhrl, Julia Herrmann, Jaroslaw Kita, Ralf Moos, and Gunter Hagen
J. Sens. Sens. Syst., 12, 205–214, https://doi.org/10.5194/jsss-12-205-2023, https://doi.org/10.5194/jsss-12-205-2023, 2023
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Sensors for detecting various gases, such as nitrogen oxides, play a major role in times of climate change in protecting the environment from the possible toxic influences of such gases. Due to their usually complex design, gas sensors may react to changes in the operating temperature, which can occur due to different ambient influences. This article shows two methods for accurately measuring the temperature on the surface of a sensor under realistic conditions.
Robin Werner, Jaroslaw Kita, Michael Gollner, Florian Linseis, and Ralf Moos
J. Sens. Sens. Syst., 12, 69–84, https://doi.org/10.5194/jsss-12-69-2023, https://doi.org/10.5194/jsss-12-69-2023, 2023
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A high-temperature gauge to simultaneously determine electrical conductivity, the Hall constant, and the Seebeck coefficient was developed. Screen-printed heating structures on a ceramic sample holder generate temperatures up to 800 °C. Heating structures were designed using FEM simulations. The temperature distribution was validated by thermal imaging. Measurements on constantan (reference material) and boron-doped silicon wafer confirm the functionality of the gauge up to 800 °C.
Johanna Distler, Thomas Wöhrl, Robin Werner, Michael Gerlach, Michael Gollner, Florian Linseis, Jaroslaw Kita, and Ralf Moos
J. Sens. Sens. Syst., 12, 9–19, https://doi.org/10.5194/jsss-12-9-2023, https://doi.org/10.5194/jsss-12-9-2023, 2023
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Differential scanning calorimetry (DSC) is a widely used tool to analyze thermal material properties. This study focuses on the advancement of a miniaturized DSC chip as an alternative to conventional devices. The first development steps for the integration of a weighing system are shown, starting with model considerations and simulation-based optimization to initial measurements. Three different measurement methods are investigated and show promising results.
Robin Werner, Jaroslaw Kita, Michael Gollner, Florian Linseis, and Ralf Moos
J. Sens. Sens. Syst., 10, 71–81, https://doi.org/10.5194/jsss-10-71-2021, https://doi.org/10.5194/jsss-10-71-2021, 2021
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A novel, low-cost measurement device for simultaneous high temperature measurements of the electrical conductivity and Hall coefficient has been developed. Simulations were used to design a suitable screen-printed planar platinum heating structure that generates temperatures of up to 600 °C. Simulations of the temperature distribution have been validated using thermal imaging. Measurements were compared with data from the literature to validate the functionality of the novel device.
Anastasiya Ruchets, Nils Donker, Jens Zosel, Daniela Schönauer-Kamin, Ralf Moos, Ulrich Guth, and Michael Mertig
J. Sens. Sens. Syst., 9, 355–362, https://doi.org/10.5194/jsss-9-355-2020, https://doi.org/10.5194/jsss-9-355-2020, 2020
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A commercial solid electrolyte gas sensor of the type "Pt|YSZ|Pt, air" based on yttria-stabilized zirconia for colorimetric oxygen detection was operated in optimized dynamic electrochemical modes. Cyclic voltammetry and square-wave voltammetry were used for the detection of NO and O2 in N2 in the temperature range between 550 and 750 °C. Due to the differences of electrode kinetics of the single components it is possible to detect these redox active gases selectively and quasi-simultaneously.
Julia Herrmann, Gunter Hagen, Jaroslaw Kita, Frank Noack, Dirk Bleicker, and Ralf Moos
J. Sens. Sens. Syst., 9, 327–335, https://doi.org/10.5194/jsss-9-327-2020, https://doi.org/10.5194/jsss-9-327-2020, 2020
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In this contribution, an inexpensive and robust impedimetric NOx sensor is presented. The impedance of a functional thick film depends selectively on the NOx concentration in the exhaust but shows a dependency on the oxygen concentration. Therefore, an additional temperature-independent resistive oxygen sensor structure was integrated on the same sensor platform. It serves not only to determine the oxygen concentration in the exhaust, but also to correct the oxygen dependency of the NOx sensor.
Nils Donker, Anastasiya Ruchets, Daniela Schönauer-Kamin, Jens Zosel, Ulrich Guth, and Ralf Moos
J. Sens. Sens. Syst., 9, 293–300, https://doi.org/10.5194/jsss-9-293-2020, https://doi.org/10.5194/jsss-9-293-2020, 2020
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Symmetrical Pt | YSZ | Pt–NO gas sensors were produced with frit-containing and fritless Pt electrodes and fired between 950 and 1300 °C. The sensors were operated by pulsed polarization. With fritless pastes, the sensors responded significantly higher. The firing temperature affects the sensitivity only slightly. The low NO sensitivity of the frit-containing electrodes was attributed to a blocking effect at the triple-phase boundaries that inhibits the oxygen transport through the sensor.
Stefanie Walter, Andreas Bogner, Gunter Hagen, and Ralf Moos
J. Sens. Sens. Syst., 8, 49–56, https://doi.org/10.5194/jsss-8-49-2019, https://doi.org/10.5194/jsss-8-49-2019, 2019
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A planar resonant radio-frequency gas sensor was equipped with an integrated heater. By simulative geometry optimization it now can be operated up to 700 °C. Sensitive materials with gas-dependent dielectric properties at higher temperatures can now be used. By coating the sensor with zeolite, ammonia could be detected. Depending on the working temperature, the sensor returns either a dosimeter signal (low temperatures) or a gas-concentration-dependent radio-frequency signal (high temperatures).
Murat Bektas, Thomas Stöcker, Angelika Mergner, Gunter Hagen, and Ralf Moos
J. Sens. Sens. Syst., 7, 289–297, https://doi.org/10.5194/jsss-7-289-2018, https://doi.org/10.5194/jsss-7-289-2018, 2018
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We prepared BaFe(1-x)-0.01Al0.01TaxO3-δ (BFATx) thick films with x between 0.1 and 0.4 at room temperature using the aerosol deposition method and we measured Seebeck coefficients and conductivities between 600 and 800 °C at different oxygen concentrations. Deposited on a transducer that includes a heater, equipotential layers, and electrode structures, a dual thermoelectric–resistive oxygen sensor with almost temperature-independent characteristics of both measurands was realized using BFAT30.
Gunter Hagen, Antonia Harsch, and Ralf Moos
J. Sens. Sens. Syst., 7, 79–84, https://doi.org/10.5194/jsss-7-79-2018, https://doi.org/10.5194/jsss-7-79-2018, 2018
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Monitoring hydrocarbon concentrations in automotive exhausts is affected by flow rate changes. The signal of thermoelectric gas sensors is a thermovoltage. Its origin is a temperature difference that depends on the flow rate. To avoid this noise effect, the sensor can be installed in a defined bypass position. As shown by simulation and experiments, the gas flow around the sensor is almost turbulence-free and the signal only depends on the hydrocarbon concentration and not on the flow rate.
Thomas Ritter, Sven Wiegärtner, Gunter Hagen, and Ralf Moos
J. Sens. Sens. Syst., 6, 395–405, https://doi.org/10.5194/jsss-6-395-2017, https://doi.org/10.5194/jsss-6-395-2017, 2017
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A planar thermoelectric gas sensor is modeled. By coupling all influences (fluid flow, gas diffusion, heat transfer, chemical reactions, and electrical properties) a model was set up that mirrors the sensor behavior precisely, as the comparison with experimental data shows. The coupling of 3-D and 1-D geometry enables to calculate the temperature distribution, fluid flow, and the gas concentration distribution in the 3-D model, while the chemical reactions are very accurately calculated in 1-D.
Franz Schubert, Michael Gollner, Jaroslaw Kita, Florian Linseis, and Ralf Moos
J. Sens. Sens. Syst., 5, 381–388, https://doi.org/10.5194/jsss-5-381-2016, https://doi.org/10.5194/jsss-5-381-2016, 2016
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An FEM model is used to improve the sensor design of a Tian–Calvet calorimeter. By modifying the basic part of the sensor (a sensor disc based on low temperature co-fired ceramics), the sensitivity was increased by a factor of 3. The model was validated and the sensors were calibrated. Indium and tin samples were measured. The melting temperatures show a deviation of 0.2 K while the enthalpy was measured with a precision better than 1 %. The values for tin deviate by less than 2 % from literature.
Franz Schubert, Michael Gollner, Jaroslaw Kita, Florian Linseis, and Ralf Moos
J. Sens. Sens. Syst., 5, 205–212, https://doi.org/10.5194/jsss-5-205-2016, https://doi.org/10.5194/jsss-5-205-2016, 2016
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Initial steps to apply a new ceramic multi-layer sensor for a Tian–Calvet calorimeter are shown. The FEM-developed sensor consists of stacked ceramic discs and insulation rings. The functionality of the sensor disc was proven up to 600 °C and the entire stack was tested at room temperature. The resolution was 5 µW and the sensitivity was 8.5 µV mW−1. The new sensor shows similar specifications as commercial devices and presents a good starting point for future high temperature applications.
F. Schubert, S. Wollenhaupt, J. Kita, G. Hagen, and R. Moos
J. Sens. Sens. Syst., 5, 25–32, https://doi.org/10.5194/jsss-5-25-2016, https://doi.org/10.5194/jsss-5-25-2016, 2016
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A manufacturing process for a planar binary lambda sensor is shown. By joining the heating and the sensing components via glass soldering with a joining temperature of 850 °C, a laboratory platform has been established that allows the manufacturing of two independent parts in HTCC technology with electrodes that are post-processed at lower temperatures, as is required for mixed-potential sensors. The concept has been proved by comparing the device with a commercial sensor.
S. Fischer, D. Schönauer-Kamin, R. Pohle, M. Fleischer, and R. Moos
J. Sens. Sens. Syst., 4, 321–329, https://doi.org/10.5194/jsss-4-321-2015, https://doi.org/10.5194/jsss-4-321-2015, 2015
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Thimble-type lambda probes that are known for their robustness in harsh exhausts can also be used as an NOx sensor by applying the pulsed polarization technique. This study evaluates in detail the influence of temperature on the NO sensitivity, so that an optimum operating point can be derived. Stepwise NO concentration changes between 0 and 12.5 ppm in synthetic exhausts demonstrate the high potential of this concept.
M. Dietrich, D. Rauch, U. Simon, A. Porch, and R. Moos
J. Sens. Sens. Syst., 4, 263–269, https://doi.org/10.5194/jsss-4-263-2015, https://doi.org/10.5194/jsss-4-263-2015, 2015
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The effect of stored ammonia on the complex dielectric permittivity of H-ZSM-5 zeolites with varying storage site density was observed between 200 and 300 °C under reaction conditions by microwave cavity perturbation. Polarization and dielectric losses were differently affected. The sensitivity of the polarization to stored ammonia is almost independent, the sensitivity of the dielectric losses strongly dependent on the storage site density. The results can be explained by proton hopping.
P. Fremerey, A. Jess, and R. Moos
J. Sens. Sens. Syst., 4, 143–149, https://doi.org/10.5194/jsss-4-143-2015, https://doi.org/10.5194/jsss-4-143-2015, 2015
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A concept to measure in situ sulfidation of silica pellet catalysts loaded with nickel is evaluated. During sulfidation between 100 and 400°C nickel sulfides form. The electrical impedance of the pellets was recorded in situ. At first, the particles are highly insulating but during sulfidation their conductivity increases by decades. Since nickel sulfides are less conductive than nickel, the strong conductivity increase may be due to conducting percolation paths that form during sulfidation.
M. Bektas, D. Hanft, D. Schönauer-Kamin, T. Stöcker, G. Hagen, and R. Moos
J. Sens. Sens. Syst., 3, 223–229, https://doi.org/10.5194/jsss-3-223-2014, https://doi.org/10.5194/jsss-3-223-2014, 2014
I. Marr, A. Groß, and R. Moos
J. Sens. Sens. Syst., 3, 29–46, https://doi.org/10.5194/jsss-3-29-2014, https://doi.org/10.5194/jsss-3-29-2014, 2014
Related subject area
Applications: Automotive and mobility
A modular adaptive residual generator for a diagnostic system that detects sensor faults on engine test beds
Inline quality monitoring of diesel exhaust fluid (AdBlue) by using the 3ω method
A novel approach for road surface wetness detection with planar capacitive sensors
A validation sensor based on carbon-fiber-reinforced plastic for early activation of automotive occupant restraint systems
Quantitative, time-resolved detection of CH4 concentrations in flows for injection analysis in CNG engines using IR absorption
Concept for completeness checking of joined structures exemplified on rail vehicle car body shells
State determination of catalytic converters based on an ultra-wideband communication system
Michael Wohlthan, Gerhard Pirker, and Andreas Wimmer
J. Sens. Sens. Syst., 11, 99–107, https://doi.org/10.5194/jsss-11-99-2022, https://doi.org/10.5194/jsss-11-99-2022, 2022
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It is a great challenge to apply a diagnostic system to engine test beds. The main problem is that such test beds involve frequent configuration changes. Therefore, the diagnostic system must be highly adaptable. A modular toolbox-based approach combines physics-based and data-driven modeling concepts and, thus, enables highly flexible application. Adaptability and detection quality are validated using measurement data from a single-cylinder engine and a multicylinder engine.
Ralf E. Bernhardsgrütter, Christoph J. Hepp, Martin Jägle, Hans-Fridtjof Pernau, Katrin Schmitt, and Jürgen Wöllenstein
J. Sens. Sens. Syst., 10, 5–12, https://doi.org/10.5194/jsss-10-5-2021, https://doi.org/10.5194/jsss-10-5-2021, 2021
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The selective catalytic reduction, an after-treatment method using diesel exhaust fluid (AdBlue), is needed to reduce the emissions of diesel combustion processes. It is crucial to monitor the diesel exhaust fluid. This article presents a platinum thin-film sensor using the 3-omega method to characterize the diesel exhaust fluid. The information about the concentration of urea in water can be extracted. The results show that this sensor can determine the urea content to within 1 % by weight.
Jakob Döring, Lakshan Tharmakularajah, Jakob Happel, and Karl-Ludwig Krieger
J. Sens. Sens. Syst., 8, 57–66, https://doi.org/10.5194/jsss-8-57-2019, https://doi.org/10.5194/jsss-8-57-2019, 2019
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This paper presents a novel approach to detect road surface wetness, which can prospectively contribute to increase the safety of vehicle passengers and traffic participants in times of highly or fully automated driving. In an experimental study, the feasibility of the approach is shown by simulating realistic road wetness scenarios on a test bench. Furthermore, a sensor system is proposed and integrated into a vehicle. The potential of the presented approach is demonstrated in a field test.
Gerald Joy Sequeira, Robert Lugner, Ulrich Jumar, and Thomas Brandmeier
J. Sens. Sens. Syst., 8, 19–35, https://doi.org/10.5194/jsss-8-19-2019, https://doi.org/10.5194/jsss-8-19-2019, 2019
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Future vehicle safety systems based on forward-looking sensors require a very robust validation system. This study describes such a validation sensor system and an algorithm to trigger safety systems in a crash. The presented sensor concept can detect the first contact and estimate the position of impact and the overlap in the initial few milliseconds of crash. The results highlight the temporal advantage of such a sensor over the present systems.
Stephan Bauke, Kai Golibrzuch, Frank Rotter, Hainer Wackerbarth, Olaf Thiele, and Thomas Berg
J. Sens. Sens. Syst., 6, 185–198, https://doi.org/10.5194/jsss-6-185-2017, https://doi.org/10.5194/jsss-6-185-2017, 2017
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This work describes the development of an optical measurement system for accurate quantification of methane (the main component of compressed natural gas) densities in gas flows based on broadband absorption of infrared light. Using various test environments we validate accuracy and precision of the quantification method. We show that our measurement system can serve as a tool for the development of modern, CO2 saving internal combustion engines reducing environmental impact of transportation.
Uwe Jurdeczka
J. Sens. Sens. Syst., 6, 53–63, https://doi.org/10.5194/jsss-6-53-2017, https://doi.org/10.5194/jsss-6-53-2017, 2017
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Completeness checking of constructional steel structures with several hundred weld-on parts still represents a great challenge. By the use of 3-D scanners, it is possible to obtain sufficiently comprehensive information about the actual configuration (as-is state). By using an adapted algorithm for post-processing of the resulting point clouds, difference figures are superimposed over the respective 3-D model as the target state. The difference figures signal the missing parts.
I. Motroniuk, R. Stöber, and G. Fischerauer
J. Sens. Sens. Syst., 4, 255–262, https://doi.org/10.5194/jsss-4-255-2015, https://doi.org/10.5194/jsss-4-255-2015, 2015
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A novel microwave-based approach for monitoring the state of aftertreatment systems such as diesel particulate filters (DPFs), three-way catalytic converters (TWCs), and selective catalytic reduction (SCR) catalysts is proposed. The interior of the catalyst metal housing serves as a communication channel between two wireless communication nodes. It is shown that, depending on the transmission channel characteristics, the properties of the catalyst, such as the catalyst state, can be inferred.
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