Articles | Volume 12, issue 2
https://doi.org/10.5194/jsss-12-215-2023
© Author(s) 2023. This work is distributed under
the Creative Commons Attribution 4.0 License.
the Creative Commons Attribution 4.0 License.
https://doi.org/10.5194/jsss-12-215-2023
© Author(s) 2023. This work is distributed under
the Creative Commons Attribution 4.0 License.
the Creative Commons Attribution 4.0 License.
Development of a gas chromatography system coupled to a metal-oxide semiconductor (MOS) sensor, with compensation of the temperature effects on the column for the measurement of ethene
Maximilian Koehne
CORRESPONDING AUTHOR
Fraunhofer Institute for Process Engineering and Packaging, 85354 Freising, Germany
Department of Systems Engineering, Saarland University, 66123 Saarbrücken, Germany
Christopher Schmidt
Fraunhofer Institute for Process Engineering and Packaging, 85354 Freising, Germany
Satnam Singh
Fraunhofer Institute for Process Engineering and Packaging, 85354 Freising, Germany
Andreas Grasskamp
Fraunhofer Institute for Process Engineering and Packaging, 85354 Freising, Germany
Tilman Sauerwald
Fraunhofer Institute for Process Engineering and Packaging, 85354 Freising, Germany
Department of Systems Engineering, Saarland University, 66123 Saarbrücken, Germany
Fraunhofer Institute for Process Engineering and Packaging, 85354 Freising, Germany
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J. Sens. Sens. Syst., 12, 93–101, https://doi.org/10.5194/jsss-12-93-2023, https://doi.org/10.5194/jsss-12-93-2023, 2023
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In this work, we have developed and validated a semi-automatic approach that greatly reduces the amount of interaction and effort needed for analyzing samples via gas chromatography–mass spectrometry. Further, unlike many other approaches, our developed tool is accessible to the novice and does not require any programming experience. Using whisky as an example substance, we show how the analysis method compares to conventional software, and we validate our approach against that.
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Applications like air quality, fire detection and detection of explosives require selective and quantitative measurements in an ever-changing background of interfering gases. One main issue hindering the successful implementation of gas sensors in real-world applications is the lack of appropriate calibration procedures for advanced gas sensor systems. This article presents a calibration scheme for gas sensors based on gas profiles with unique randomized gas mixtures.
Caroline Schultealbert, Iklim Uzun, Tobias Baur, Tilman Sauerwald, and Andreas Schütze
J. Sens. Sens. Syst., 9, 283–292, https://doi.org/10.5194/jsss-9-283-2020, https://doi.org/10.5194/jsss-9-283-2020, 2020
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We present a work on gas sensors that can for example be used for the assessment of indoor air quality. These sensors suffer from deterioration by siloxanes, so we investigated these effects by a distinct operation mode and exposition to this gas that allows us to interpret different reactions on the sensor surface. We found that all processes on the sensor surface are slowed down by this treatment and a self-compensation by the evaluation of oxygen adsorption processes is likely to be found.
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J. Sens. Sens. Syst., 8, 261–267, https://doi.org/10.5194/jsss-8-261-2019, https://doi.org/10.5194/jsss-8-261-2019, 2019
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J. Sens. Sens. Syst., 8, 161–169, https://doi.org/10.5194/jsss-8-161-2019, https://doi.org/10.5194/jsss-8-161-2019, 2019
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J. Sens. Sens. Syst., 7, 411–419, https://doi.org/10.5194/jsss-7-411-2018, https://doi.org/10.5194/jsss-7-411-2018, 2018
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A novel method for the detection of short pulses of gas at very low concentrations is presented. Applying the method to a doped SnO2 detector, gas pulses down to a dosage of 1 ppb times seconds can be detected. The gas transport inside the detector is simulated using the finite element method (FEM) to optimize the gas transport and to keep response and recovery time as short as possible. With this approach, we have demonstrated a detection limit for ethanol below 47 fg.
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J. Sens. Sens. Syst., 7, 235–243, https://doi.org/10.5194/jsss-7-235-2018, https://doi.org/10.5194/jsss-7-235-2018, 2018
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Martin Leidinger, Joni Huotari, Tilman Sauerwald, Jyrki Lappalainen, and Andreas Schütze
J. Sens. Sens. Syst., 5, 147–156, https://doi.org/10.5194/jsss-5-147-2016, https://doi.org/10.5194/jsss-5-147-2016, 2016
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M. Schüler, T. Sauerwald, and A. Schütze
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Short summary
Continuous inspection of gases is increasingly important for process monitoring, like fruit ripening. This involves the detection of individual markers in complex gas mixtures, e.g., to indicate spoilage. Unfortunately, classical techniques are lab-bound and resource-intensive. Hence, small, low-cost systems are being developed. Thereto, we propose a sensor system, containing a non-heated gas separation unit and gas sensors combined with a compensation of surrounding temperature effects.
Continuous inspection of gases is increasingly important for process monitoring, like fruit...