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Symmetrical Pt | YSZ | Pt–NO gas sensors were produced with frit-containing and fritless Pt electrodes and fired between 950 and 1300 °C. The sensors were operated by pulsed polarization. With fritless pastes, the sensors responded significantly higher. The firing temperature affects the sensitivity only slightly. The low NO sensitivity of the frit-containing electrodes was attributed to a blocking effect at the triple-phase boundaries that inhibits the oxygen transport through the sensor.
JSSS | Articles | Volume 9, issue 2
J. Sens. Sens. Syst., 9, 293–300, 2020
https://doi.org/10.5194/jsss-9-293-2020

Special issue: Dresden Sensor Symposium DSS 2019

J. Sens. Sens. Syst., 9, 293–300, 2020
https://doi.org/10.5194/jsss-9-293-2020

Regular research article 17 Sep 2020

Regular research article | 17 Sep 2020

Influence of Pt paste and the firing temperature of screen-printed electrodes on the NO detection by pulsed polarization

Nils Donker et al.

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Cited articles

Bay, L. and Jacobsen, T.: Dynamics of the YSZ-Pt interface, Solid State Ionics, 93, 201–206, https://doi.org/10.1016/S0167-2738(96)00526-7, 1997. 
Bhatia, D., McCabe, R. W., Harold, M. P., and Balakotaiah, V.: Experimental and kinetic study of NO oxidation on model Pt catalysts, J. Catal., 266, 106–119, https://doi.org/10.1016/j.jcat.2009.05.020, 2009. 
Donker, N., Ruchets, A., Schönauer-Kamin, D., Zosel, J., Guth, U., and Moos, R.: Influence of polarization time and polarization current of Pt|YSZ-based NO sensors utilizing the pulsed polarization when applying constant charge, Sensor. Actuat. B, 290, 28–33, https://doi.org/10.1016/j.snb.2019.03.060, 2019. 
Fischer, S., Pohle, R., Farber, B., Proch, R., Kaniuk, J., Fleischer, M., and Moos, R.: Method for detection of NOx in exhaust gases by pulsed discharge measurements using standard zirconia-based lambda sensors, Sensor. Actuat. B, 147, 780–785, https://doi.org/10.1016/j.snb.2010.03.092, 2010. 
Fischer, S., Pohle, R., Magori, E., Fleischer, M., and Moos, R.: Detection of NO by pulsed polarization of Pt I YSZ, Solid State Ionics, 262, 288–291, https://doi.org/10.1016/j.ssi.2014.01.022, 2014. 

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Short summary
Symmetrical Pt | YSZ | Pt–NO gas sensors were produced with frit-containing and fritless Pt electrodes and fired between 950 and 1300 °C. The sensors were operated by pulsed polarization. With fritless pastes, the sensors responded significantly higher. The firing temperature affects the sensitivity only slightly. The low NO sensitivity of the frit-containing electrodes was attributed to a blocking effect at the triple-phase boundaries that inhibits the oxygen transport through the sensor.
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